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Hola forero.
La literatura sobre la preparación de nitroalcanos es bastante extensa y te dejo algunos links, para que te convenzas de ello:
www.organic-chemistry.org/synthesis/C1N/nitro-compounds.shtm
pubs.acs.org/doi/abs/10.1021/ja01645a007
www.organic-chemistry.org/synthesis/C1C/...nitro-compounds.shtm
erowid.org/archive/rhodium/chemistry/nitroalkane.html
books.google.com.bo/books?id=XmBZAvILOKA...%20synthesis&f=false
cameprints.unicam.it/281/1/PhD_THESIS_CO...SERENA_GABRIELLI.pdf

Saludos.